Furthermore, the volatile changes were tested by differential thermal gravimetric analysis. 通过差热热重分析法检验包合物的挥发性变化情况。
These ligands which coordinate with transition metal in suitable solvent and washings by water, can be synthesized 10 coordination compounds. Their compositions are asserted by elementary organic analysis, ICP emission spectrum 、 differential thermal gravimetric analysis. 配体在适当的溶剂中与过渡金属配合,然后经水洗涤,得到10个配合物,经过元素分析、ICP发射光谱分析、热失重分析确定了它们的组成。
Based on the characteristic temperature of the differential thermal curves for different minerals, the ignition temperature for differential thermal and thermo gravimetric difference analysis of total carbon, carbon dioxide, water crystal and sulfur in sulfides etc. 根据矿物差热曲线特征温度,拟定使用热重差分析岩矿中全碳、结晶水、硫化物硫和二氧化碳等项目的灼烧温度范围,并进行热重差分析。
The samples were characterized by X-ray diffraction ( XRD ) Differential Thermal Analysis and Thermo Gravimetric Analysis ( DTA-TG ) and Transmission Electron Microscopy ( TEM ). 利用热分析仪(TG-DTA)、透射电子显微镜(TEM)、X射线衍射仪(XRD)对材料的结构进行表征。
The thin films of InVO_4 doped by Ni under control were prepared by sol-gel method, crystal structure of InVO_4 and the synthesis process were characterized by X-ray diffractometry ( XRD ), differential thermal analysis associated with thermal gravimetric analysis ( TGA-DTA ). 采用溶胶凝胶(sol-gel)法制备Ni控制掺杂的InVO4可见光催化剂薄膜。通过X射线衍射分析、差热热重分析确定InVO4晶体结构及合成工艺;